Electrochemical Fluorination of (Arylthio)methyl Carboxylates and γ–Phenylthio–γ–butyrolactone Derivative / Satoshi Ito; Kaori Kondo; Hideki Ishii; Shinsuke Inagi; Toshio Fuchigami
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© 2021 The Electrochemical Society ("ECS"). Published on behalf of ECS by IOP Publishing Limited.Electrochemical fluorination of various (arylthio)methyl carboxylates was carried out in aprotic organic solvents containing poly(HF) salts to provide the corresponding O–fluoromethyl carboxylates in good to moderate yield. Electrochemical fluorination of a cyclic analogue, a γ–phenylthio–γ–butyrolactone derivative was also achieved under ultrasonication to give the corresponding 4–fluorinated product in moderate yield.
